Chloroacetamide Typical Properties
Item
Specifications
Results
Appearance
White crystalline powder
White crystalline powder
Acidity %
≤0.08
0.06
Melting range ℃
116-122
118.0-119.1
Water content(by KF) %
≤0.20
0.06
Purity(by HPLC) %
≥99
99.32
Ammonium Chloride Assay %
≤0.5
0.05
Conclusion
The results conforms with Enterprise standards
Chloroacetamide Usage
Used for synthesis of chloroacetonitrile sulfameprazine and other organic compounds used in organic synthesis, pharmaceutical intermediates and synthesis of chloroacetonitrile sulfameprazine 3-methoxypyrazine and other organic compounds.
production method
Derived from the reaction of ethyl chloroacetate and ammonia. First cool ethyl chloroacetate to below 10 ℃, slowly add ammonia water (relative density 0.9) with stirring, and white crystals precipitate immediately.
After adding ammonia, continue to stir for 1h, filter out the crystals, wash off the ammonium chloride with ammonia, try to filter it out to be the crude product, and then recrystallize with ethanol to get the finished product.
Chloroacetamide Packaging and Shipping
Packing: 25kg/drum
Chloroacetamide Storage
Stored in cool dry ventilated place away from fire, heat, light, acids and food materials
