1-Bromotetradecane Typical Properties
Item
Method of Analysis
Standard
Result
appearance
visual inspection
Colorless transparent liquid
Colorless transparent liquid
Purity
gas chromatography
≥99.0%
99.36%
moisture
–
＜0.05%
0.038%
1-Bromotetradecane Usage
Used in organic synthesis, can be used in the synthesis of medicine and other fine chemicals.
production method
Derived from tetradecanol by bromination.
Add myristyl alcohol to the reaction pot, add sulfuric acid dropwise with stirring, and continue stirring for half an hour after the addition.
Then add hydrobromic acid, heat to 99-101 ℃, and react for 8h. Cool to 30 ° C, stop stirring, leave for 12h, separate the upper oily substance, and adjust the pH to 8 with 10% sodium carbonate solution.
Separate the water layer, and wash the oil twice with an equal volume of 50% ethanol. Add the washed oil to sodium carbonate, stir intermittently, and dry for 24 hours. Filter to get the finished product.
1-Bromotetradecane Packing
25kgs/drum
1-Bromotetradecane Storage
1-Bromotetradecane should be stored in a closed system, and be kept in a dry dark place without any light exposure. The shelf life is two years in original, unopened containers.
